Novel Developments in Pharmaceutical and Biomedical Analysis

Book Series: Recent Advances in Analytical Techniques

Volume 2

by

Atta-ur-Rahman, Sibel A. Ozkan, Rida Ahmed

DOI: 10.2174/97816810857461180201
eISBN: 978-1-68108-574-6, 2018
ISBN: 978-1-68108-575-3
ISSN: 2542-5617 (Print)
ISSN: 2542-5625 (Online)



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Recent Advances in Analytical Techniques is a series of updates in techniques used in chemical analysis. Each volume ...[view complete introduction]
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Table of Contents

Preface

- Pp. i
Atta-ur- Rahman, Sibel A. Ozkan and Rida Ahmed
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List of Contributors

- Pp. ii-iii (2)
Atta-ur- Rahman, Sibel A. Ozkan and Rida Ahmed
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Advances in Validated Chromatographic Assay of Solid Dosage Forms and Their Drug Dissolution Studies

- Pp. 1-43 (43)
Sevinc Kurbanoglu, Ozgur Esim, Ayhan Savaser, Sibel A. Ozkan and Yalcin Ozkan

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Novel Validated UHPLC Method for the Estimation of Drug Active Compounds

- Pp. 44-97 (54)
Mehmet Gumustas, Bengi Uslu and Sibel A. Ozkan

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HILIC Based LC/MS for Metabolite Analysis

- Pp. 98-130 (33)
Emirhan Nemutlu and Sedef Kır

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In Vitro Methods for the Evaluation of Oxidative Stress

- Pp. 131-172 (42)
Hande Gurer Orhan, Sibel Suzen, Tamas Balint Csont, Miroslav Pohanka, Bozena Nejman-Falenczyk, Grzegorz Wegrzyn and Luciano Saso

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The Application of Vibrational Spectroscopy in Studies of Structural Polymorphism of Drugs

- Pp. 173-207 (35)
Przemysław Zalewski, Gabriela Wiergowska, Joanna Goscianska, Kornelia Lewandowska and Judyta Cielecka-Piontek

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Electrochemical Biosensors Based on Conductive Polymers and Their Applications in Biomedical Analysis

- Pp. 208-248 (41)
Sławomira Skrzypek and Paweł Krzyczmonik

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New Trends in Electrochemical Sensors Modified with Carbon Nanotubes and Graphene for Pharmaceutical Analysis

- Pp. 249-301 (53)
Burcin Bozal-Palabiyik, Burcu Dogan-Topal, Sibel A. Ozkan and Bengi Uslu

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Electrochemical Nanobiosensors in Pharmaceutical Analysis

- Pp. 302-353 (52)
Sevinc Kurbanoglu, Sibel A. Ozkan and Arben Merkoci

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Optical Sensor Arrays for Pharmaceutical and Biomedical Analyses

- Pp. 354-381 (28)
Pavel Anzenbacher and Mehmet Gokhan Caglayan

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Applications of Ionic Liquids in Chemical Science

- Pp. 382-412 (31)
Imran Ali, Zeid A. Alothman, Abdulrahman Alwarthan and Hassan Y. Aboul-Enein

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New Trends in Enantioanalysis of Pharmaceutical Compounds using Electrochemical Sensors

- Pp. 413-432 (20)
Raluca-Ioana Stefan-van Staden

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Subject Index

- Pp. 433-451 (19)
Atta-ur- Rahman, Sibel A. Ozkan and Rida Ahmed
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Preface

“Recent Advances in Analytical Techniques Vol. 2, “Novel Developments in Pharmaceutical and Biomedical Analysis” presents important recent developments in various analytical methods covering such fields as electrochemistry, optical sensor arrays for pharmaceutical and biomedical analysis, FTIR, high performance liquid chromatographic analysis, chiral separation and other techniques.

The first three chapters cover separation techniques including chromatographic assay of solid dosage forms of drugs, UHPLC method for the estimation of drug active compounds; and HILIC based LC/MS for metabolite analysis. The next chapter presents in vitro methods for the evaluation of oxidative stress; while chapter 5 describes the applications of vibrational spectroscopy in studies of structural polymorphism of drugs. Electrochemical biosensors based on conductive polymers and their applications in biomedical analysis are presented in chapter 6 while chapter 7 discusses new trends in electrochemical sensors modified with carbon nanotubes and graphene for pharmaceutical analysis. Chapter 8 describes the use of electrochemical nanobiosensors in pharmaceutical analysis while the next chapter discusses optical sensor arrays for pharmaceutical and biomedical analyses. The applications of ionic liquids in chemical science are discussed in chapter 10 whereas new trends in enantioanalysis of pharmaceutical compounds using electrochemical sensorsare presented in the last chapter.

We are deeply grateful to all the authors for their excellent contributions which should be of wide interest to the readers. We are also grateful to Mr. Mahmood Alam (Director Publications) and his excellent team comprising Mr. Shehzad Naqvi (Senior Manager Publications) and Mr. Omer Shafi (Assistant Manager Publications) for their untiring efforts.

Atta-ur-Rahman, FRS
International Centre for Chemical and Biological Sciences,
University of Karachi,
Karachi 75270,
Pakistan

Sibel A. Ozkan
Faculty of Pharmacy,
Department of Analytical Chemistry,
Ankara University,
06560 Yenimahalle/Ankara,
Turkey

&

Rida Ahmed
TCM and Ethnomedicine Innovation & Development Laboratory,
School of Pharmacy,
Hunan University of Chinese Medicine,
Changsha 410208,
P.R. China

List of Contributors

Editor(s):
Atta-ur-Rahman
Kings College
University of Cambridge
Cambridge
UK


Sibel A. Ozkan
Department of Basic Pharmaceutical Sciences
Ankara University
06560 Yenimahalle/Ankara
Turkey


Rida Ahmed
TCM and Ethnomedicine Innovation & Development Laboratory, School of Pharmacy
Hunan University of Chinese Medicine
Changsha 410208
P.R. China




Contributor(s):
Abdulrahman Alwarthan
Department of Chemistry, College of Science
King Saud University
Riyadh
Kingdom of Saudi Arabia


Arben Merkoçi
Nanobioelectronics and Biosensors Group, Catalan Institute of Nanoscience and Nanotechnology (ICN2)
CSIC and The Barcelona Institute of Science and Technology, Campus UAB
Barcelona
Spain
/
ICREA
Pg. Lluís Companys
Barcelona
Spain


Ayhan Savaser
Department of Pharmaceutical Technology
University of Health Sciences
Gulhane Campus, Etlik
Turkey


Bengi Uslu
Faculty of Pharmacy, Department of Analytical Chemistry
Ankara University
Tandogan, Ankara
Turkey


Bożena Nejman-Faleńczyk
Department of Molecular Biology
University of Gdansk
Gdansk
Poland


Burcin Bozal-Palabiyik
Faculty of Pharmacy, Department of Analytical Chemistry
Ankara University
Ankara
Turkey


Burcu Dogan-Topal
Faculty of Pharmacy, Department of Analytical Chemistry
Ankara University
Ankara
Turkey


Emirhan Nemutlu
Faculty of Pharmacy, Department of Analytical Chemistry
Hacettepe University
Ankara
Turkey


Gabriela Wiergowska
Department of Pharmaceutical Chemistry, Faculty of Pharmacy
Poznan University of Medical Sciences
Poznań
Poland
/
PozLab sp. z o.o. (Contract Research Organization) Parkowa 2
Poznań
Poland


Grzegorz Węgrzyn
Department of Molecular Biology
University of Gdansk
Gdansk
Poland


Hande Gürer Orhan
Faculty of Pharmacy, Department of Toxicology
University of Ege
Izmir
Turkey


Hassan Y. Aboul-Enein
Pharmaceutical and Medicinal Chemistry Department, Pharmaceutical and Drug Industries Research Division
National Research Centre
Giza
Egypt


Imran Ali
Department of Chemistry
Jamia Millia Islamia (Central University)
New Delhi
India


Joanna Goscianska
Laboratory of Applied Chemistry, Faculty of Chemistry
Adam Mickiewicz University in Poznań
Poznań
Poland


Judyta Cielecka-Piontek
Department of Pharmaceutical Chemistry, Faculty of Pharmacy
Poznan University of Medical Sciences
Poznań
Poland


Kornelia Lewandowska
Polish Academy of Science, Mariana Smoluchowskiego
Institute of Molecular Physics
Poznań
Poland


Luciano Saso
Faculty of Pharmacy and Medicine
Department of Physiology and Pharmacology “Vittorio Erspamer”
Rome
Italy


Mehmet Gokhan Caglayan
Faculty of Pharmacy, Department of Analytical Chemistry
Ankara University
Ankara
Turkey


Mehmet Gumustas
Faculty of Pharmacy, Department of Analytical Chemistry
Ankara University
Tandogan, Ankara
Turkey
/
Faculty of Arts & Sciences, Department of Chemistry
Hitit University
Corum
Turkey


Ozgur Esim
Faculty of Pharmacy, Department of Analytical Chemistry
Ankara University
Tandogan, Ankara
Turkey


Pavel Anzenbacher Jr
Center for Photochemical Sciences and Department of Chemistry
Bowling Green State University
Bowling Green, OH
USA


Paweł Krzyczmonik
Department of Inorganic and Analytical Chemistry
University of Łódź
Łódź
Poland


Przemysław Zalewski
Department of Pharmaceutical Chemistry, Faculty of Pharmacy
Poznan University of Medical Sciences
Poznań
Poland


Raluca-Ioana Stefan-van Staden
Laboratory of Electrochemistry and PATLAB Bucharest
National Institute of Research for Electrochemistry and Condensed Matter
Bucharest
Romania


Sedef Kır
Faculty of Pharmacy, Department of Analytical Chemistry
Hacettepe University
Ankara
Turkey


Sevinc Kurbanoglu
Faculty of Pharmacy, Department of Analytical Chemistry
Ankara University
Tandogan, Ankara
Turkey
/
Nanobioelectronics and Biosensors Group, Catalan Institute of Nanoscience and Nanotechnology (ICN2)
CSIC and The Barcelona Institute of Science and Technology, Campus UAB
Barcelona
Spain


Sibel A. Ozkan
Faculty of Pharmacy, Department of Analytical Chemistry
Ankara University
Tandogan, Ankara
Turkey


Sibel Suzen
Faculty of Pharmacy, Department of Pharmaceutical Chemistry
University of Ankara
Tandogan, Ankara
Turkey


Sławomira Skrzypek
Department of Inorganic and Analytical Chemistry
University of Łódź
Łódź
Poland


Tamás Bálint Csont
Faculty of General Medicine, Department of Biochemistry
University of Szeged
Szeged
Hungary


Yalcin Ozkan
Department of Pharmaceutical Technology
University of Health Sciences
Gulhane Campus, Etlik
Turkey


Zeid A. Alothman
Department of Chemistry, College of Science
King Saud University
Riyadh
Kingdom of Saudi Arabia




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