Editors: M. Valcárcel, S. Cárdenas, R. Lucena

Analytical Microextraction Techniques

eBook: US $99 Special Offer (PDF + Printed Copy): US $192
Printed Copy: US $143
Library License: US $396
ISBN: 978-1-68108-380-3 (Print)
ISBN: 978-1-68108-379-7 (Online)
Year of Publication: 2016
DOI: 10.2174/97816810837971170101

Introduction

Sample treatment has been the focus of intensive research in the last 20 years since it still remains a bottleneck in precise analytical procedures. The low concentration of the target analytes, the large amount of potential interfering agents and the incompatibility of the sample matrix with the instrumental techniques are the main reasons for these bottlenecks. In most of these methods, sample treatment is an unavoidable step and it has a clear influence on the quality (sensitivity, selectivity, and accuracy) of the final analytical results.

While the usefulness of microextraction techniques has been established, their complete acceptance in analytical laboratories (including official methods of analysis) depends on their successful automation and integration with conventional analytical instrumentation.

Analytical Microextraction Techniques presents comprehensive information about several analytical methods that are useful in the laboratory. These include: sorptive microextraction, solid and liquid phase microextraction, packed sorbent microextraction, miniaturized dispersive solid-phase extraction, thin film and nanoparticle based techniques, and membrane-based techniques.

This is a vital reference on microextraction and sample preparation techniques for applied chemistry students, analytical chemists and laboratory technicians.

Foreword

- Pp. i-ii (2)
Stig Pedersen-Bjergaard
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Preface

- Pp. iii-iv (2)
Miguel Valcárcel, Soledad Cárdenas, Rafael Lucena
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List of Contributors

- Pp. v-vii (3)
Miguel Valcárcel, Soledad Cárdenas, Rafael Lucena
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Green Microextraction

- Pp. 3-27 (25)
Sergio Armenta, Miguel de la Guardia, Jacek Namiesnik
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Novel Sol-Gel Sorbents in Sorptive Microextraction

- Pp. 28-69 (42)
Abuzar Kabir, Kenneth G. Furton
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Ionic Liquids in the Microextraction Context

- Pp. 70-134 (65)
María J. Trujillo-Rodríguez, Verónica Pino, Juan H. Ayala, Ana M. Afonso
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Application of Nanomaterials in Solid and Liquid Microextraction

- Pp. 135-166 (32)
Yolanda Moliner-Martínez, Pascual Serra-Mora, Jorge Verdú-Andrés, Carmen Molins-Legua, Rosa Herráez-Hernández, Pilar Campíns-Falcó
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Principles and Developments of Solid-Phase Microextraction

- Pp. 167-218 (52)
Adam Kloskowski, Łukasz Marcinkowski, Francisco Pena-Pereira, Jacek Namieśnik
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Stir Bar Sorptive Extraction and Related Techniques

- Pp. 219-240 (22)
José Manuel Florêncio Nogueira
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Microextraction by Packed Sorbent (MEPS): Theory, Developments and Applications

- Pp. 241-253 (13)
Mohammad Mahdi Moein, Abbi Abdel-Rehim, Mohamed Abdel-Rehim
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Miniaturized Dispersive Solid-phase Extraction

- Pp. 254-276 (23)
Guillermo Lasarte-Aragonés, Rafael Lucena, Soledad Cárdenas, Miguel Valcárcel
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Solid Phase Extraction Based on Magnetic Nanoparticles

- Pp. 277-305 (29)
Ángel Ríos, Mohammed Zougagh
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Solid-Phase Microextraction Under the Thin Film Format

- Pp. 306-326 (21)
M. Roldán-Pijuán, R. Lucena, S. Cárdenas, M. Valcárcel
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Single-drop Microextraction and Related Techniques

- Pp. 327-379 (53)
Francisco Pena-Pereira, Isela Lavilla, Carlos Bendicho
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Membrane-Based Microextraction Techniques with Emphasis on Hollow-fiber Microextraction

- Pp. 380-405 (26)
Jan Åke Jönsson, Estelle Larsson
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Subject Index

- Pp. 406-414 (9)
Miguel Valcárcel, Soledad Cárdenas, Rafael Lucena
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